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Beilstein J. Org. Chem. 2018, 14, 2375–2383, doi:10.3762/bjoc.14.213
Graphical Abstract
Figure 1: Functional molecules with CF2CF2-fragment.
Scheme 1: Preparation and synthetic applications of 2-Zn.
Figure 2: Recovery yield of 2-Zn in DMF (ca. 0.70 M) after stirring at various temperature conditions.
Figure 3: Copper(I)-catalyzed cross-coupling reaction of 2-Zn with various iodoarene derivatives. NMR (isolat...
Scheme 2: Multigram-scale cross-coupling of 2-Zn with iodoarenes.
Scheme 3: Synthesis of a CF2CF2 group containing tolane derivative.
Figure 4: Copper(I)-catalyzed cross-coupling reaction of 2-Zn with various acid chlorides. NMR yields (isolat...